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Microwave-assisted synthesis and bioevaluation of new sulfonamides

Journal of Enzyme Inhibition and Medicinal Chemistry · Ocak 2017

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YÖKSİS Kayıtları
Microwave-assisted synthesis and bioevaluation of new sulfonamides
Journal of Enzyme Inhibition and Medicinal Chemistry · 2017 SCI-Expanded
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Makale Bilgileri

DergiJournal of Enzyme Inhibition and Medicinal Chemistry
Yayın TarihiOcak 2017
Cilt / Sayfa32 · 369-374
Erişim🔓 Açık Erişim
Özet In this study, 4-[5-(4-hydroxyphenyl)-3-aryl-4,5-dihydro-1H-pyrazol-1-yl]benzenesulfonamide derivatives (8-14) were synthesized for the first time by microwave irradiation and their chemical structures were confirmed by 1H NMR, 13C NMR and HRMS. Cytotoxic activities and inhibitory effects on carbonic anhydrase I and II isoenzymes of the compounds were investigated. The compounds 9 (PSE = 4.2), 12 (PSE = 4.1) and 13 (PSE = 3.9) with the highest potency selectivity expression (PSE) values in cytotoxicity experiments and the compounds 13 (Ki = 3.73 ± 0.91 nM toward hCA I) and 14 (Ki = 3.85 ± 0.57 nM toward hCA II) with the lowest Ki values in CA inhibition studies can be considered as leader compounds for further studies.

Yazarlar (8)

1
H. I. Gul
2
Cem Yamali
ORCID: 0000-0002-4833-7900
3
Fatma Yesilyurt
4
H. Sakagami
5
Kaan Kucukoglu
ORCID: 0000-0001-8977-9775
6
Gülçin
7
Mustafa Gul
8
Claudiu T. Supuran
ORCID: 0000-0003-4262-0323

Anahtar Kelimeler

Carbonic anhydrase cytotoxicity microwave pyrazoline sulfonamide

Kurumlar

Atatürk Üniversitesi
Erzurum Turkey
Ataturk University, Faculty of Medicine
Erzurum Turkey
College of Sciences
Riyadh Saudi Arabia
Meikai University
Sakado Japan
Università degli Studi di Firenze
Florence Italy

Metrikler

46
Atıf
8
Yazar
5
Anahtar Kelime

Sistemimizdeki Yazarlar