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Design, synthesis, molecular modeling, DFT, ADME and biological evaluation studies of some new 1,3,4-oxadiazole linked benzimidazoles as anticancer agents and aromatase inhibitors

Journal of Biomolecular Structure and Dynamics · Ocak 2023

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YÖKSİS Kayıtları
Design, synthesis, molecular modeling, DFT, ADME and biological evaluation studies of some new 1,3,4-oxadiazole linked benzimidazoles as anticancer agents and aromatase inhibitors
Journal of Biomolecular Structure and Dynamics · 2022 SCI-Expanded
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Makale Bilgileri

DergiJournal of Biomolecular Structure and Dynamics
Yayın TarihiOcak 2023
Cilt / Sayfa41 · 1944-1958
Özet Breast cancer is the most frequent female cancer and second cause of cancer-related deaths among women around the world. Two thirds of breast cancer patients have hormone-dependent tumors, which is very likely be treated with hormonal therapy. Aromatase is involved in the biosynthesis of estrogen thus a critical target for breast cancer. In this study, in order to identify new aromatase enzyme inhibitors, a series of benzimidazole-1,3,4-oxadiazole derivatives were synthesized and characterized by 1H NMR, 13C NMR, and MS spectra analyses. In the in vitro anticancer assay, all the compounds tested anticancer activities using MTT-based assay against five cancer cell lines (MCF-7, A549, HeLa, C6, and HepG2). Among them, compound 5a exhibited the most potent activity with IC50 values of 5.165 ± 0.211 μM and 5.995 ± 0.264 μM against MCF-7 and HepG2 cell lines. Compound 5a was included in the BrdU test to determine the DNA synthesis inhibition effects for both cell types. Furthermore, compound 5c was also found to be more effective than doxorubicin on the HeLa cell line. The selectivity of anticancer activity was evaluated in NIH3T3 cell line. In vitro, enzymatic inhibition assays of aromatase enzyme were performed for compound 5a acting on the MCF-7 cell line. For compound 5a, in silico molecular docking and dynamics simulations against aromatase enzyme was performed to determine possible protein-ligand interactions and stability. DFT study was performed to evaluate the quantum mechanical and electronic properties of compound 5a. Finally, the theoretical ADME properties of the potential aromatase inhibitor compound 5a were analyzed by calculations. Communicated by Ramaswamy H. Sarma.

Yazarlar (7)

1
Ulviye Acar Çevik
ORCID: 0000-0003-3537-2544
2
Ismail Celik
ORCID: 0000-0002-8146-1663
3
Ayşen Işık
4
Iqrar Ahmad
5
Harun Patel
ORCID: 0000-0003-0920-1266
6
Yusuf Özkay
7
Zafer Asım Kaplancıklı

Anahtar Kelimeler

ADME aromatase Benzimidazole DFT docking dynamics

Kurumlar

Anadolu Üniversitesi
Eskisehir Turkey
Erciyes Üniversitesi
Kayseri Turkey
R. C. Patel Institute of Pharmaceutical Education and Research
Shirpur India
Selçuk Üniversitesi
Selçuklu Turkey

Metrikler

50
Atıf
7
Yazar
6
Anahtar Kelime