Thermal degradation behaviour of NI(II) complex of 3,4- methylenedioxaphenylaminoglyoxime

Journal of Chemistry · Aralık 2013

YÖKSİS Kayıtları

Thermal Degradation Behaviour of Ni II Complex of 3 4 Methylenedioxaphenylaminoglyoxime

Journal of Chemistry · 2013 SCI-Expanded

Prof. Dr. PERVİN SOYLU →

YÖKSİS Kayıtları — ISSN Eşleşmesi

Thermal Degradation Behaviour of Ni II Complex of 3 4 Methylenedioxaphenylaminoglyoxime

2013 ISSN: 2090-9063 SCI-Expanded

Prof. Dr. PERVİN SOYLU →

10.1155/2013/548067

Synthesis and Antimicrobial Assessment of Fe3 InclusionComplex of p-tert-Butylcalix[4]arene Diamide Derivative

2019 ISSN: 2090-9063 SCI-Expanded

Dr. Öğr. Üyesi FATİH DURMAZ →

10.1155/2019/2534072

Makale Bilgileri

Dergi Journal of Chemistry

ISSN20909063

Yayın TarihiAralık 2013

DOI10.1155/2013/548067

Scopus ID2-s2.0-84888862123

Erişim🔓 Açık Erişim

Özet Thermal degradation behaviour of the Ni(II) complex of 3,4- methylenedioxaphenylaminoglyoxime was investigated by TG, DTA, and DTG at a heating rate of 10°C min-1 under dinitrogen. The acquired experimental data shows that the complex is thermally stable up to 541 K. The pyrolytic decomposition process occurs by melting metal complex and metal oxide remains as final product. The energies of the reactions involved and the mechanism of decomposition at each stage have been examined. The values of kinetic parameters such as activation energy (E), preexponential factor (A) and thermodynamic parameters such as enthalpy (Δ H), entropy (Δ S), and Gibbs free energy (Δ G) are also evaluated. © 2013 Emin Karapinar et al.