Scopus
YÖKSİS Eşleşti
Simultaneous determination of some basic dyes using p-tetranitrocalix[4] arene-appended silica-based HPLC column
Analytical Methods · Eylül 2014
YÖKSİS Kayıtları
Simultaneous determination of some basic dyes using p-tetranitrocalix[4]arene-appended silica-based HPLC column
Analytical Methods · 2014 SCI-Expanded
DOKTOR ÖĞRETİM ÜYESİ FATİH DURMAZ →
Makale Bilgileri
DergiAnalytical Methods
Yayın TarihiEylül 2014
Cilt / Sayfa6 · 7318-7323
Scopus ID2-s2.0-84906673990
Özet
This study focuses on the synthesis, characterization and application of p-tetranitrocalix[4]arene-appended silica-based material as a stationary phase in high-performance liquid chromatography for the simultaneous separation of some basic dyes such as methyl violet, methyl green and methylene blue. The effect of the pH of mobile phase on the retention, separation and selectivity of these compounds was investigated. The method was validated for system efficiency, linearity, accuracy, precision, limit of detection and quantification. The limits of detection were 0.1, 0.5 and 0.3 mg L-1; whereas, the limits of quantification were observed to be 1, 1.2 and 0.9 mg L-1 for methyl violet, methyl green and methylene blue, respectively. The separation efficiency of the p-tetranitrocalix[4]arene-appended silica-based column was also compared to that of the octadecylsilane column. © the Partner Organisations 2014.
Yazarlar (6)
1
Shahabuddin Memon
2
Fakhar N. Memon
ORCID: 0000-0002-8700-5597
3
Fatih Durmaz
4
Naeem A. Memon
5
Ayaz A. Memon
6
Huseyin Kara
Kurumlar
Necmettin Erbakan Üniversitesi
Meram Turkey
Selçuk Üniversitesi
Selçuklu Turkey
University of Sindh
Jamshoro Pakistan
Metrikler
11
Atıf
6
Yazar